Revista de Odontologia da UNESP
https://revodontolunesp.com.br/article/doi/10.1590/1807-2577.10118
Revista de Odontologia da UNESP
Original Article

Bond and topography evaluation of a Y-TZP ceramic with a superficial low-fusing porcelain glass layer after different hydrofluoric acid etching protocols

Avaliação da adesão e topografia de uma zircônia Y-TZP com uma camada de glaze após diferentes protocolos de condicionamento com ácido fluorídrico

Arthur Chaves SIMÕES; Jean Soares MIRANDA; Rodrigo Othávio de Assunção e SOUZA; Estevão Tomomitsu KIMPARA; Fabíola Pessôa Pereira LEITE

http://dx.doi.org/10.1590/1807-2577.10118 Rev. odontol. UNESP, vol.47, n6, p.0, 2018
PDF
Downloads: 1
Views: 727

Abstract

Abstract: Introduction: Despite being one of the most studied ceramics today, zirconia still does not have a well-defined adhesion protocol.

Objective: Evaluate the influence of different etching times and hydrofluoric acid (HF) concentrations on the zirconia surface and bond strength between a vitrified Y-TZP ceramic and a resin cement.

Materials and method: The zirconia surface treatments were: sandblasting with silica-coated alumina (Co); glaze application + 5% HF etching for 5s (G5-5s), 10s (G5-10s) or 20s (G5-20s); glaze application + 10% HF etching for 5s (G10-5s), 10 (G10-10s) or 20s (G10-20s) . Then, cement cylinders (3.3 × 3.3 mm) were built up for shear bond test on all specimens. The specimens were subjected to 6000 thermal cycling before the test. Fractures were analyzed by stereomicroscope. Data were statistically analyzed by Kruskal-Wallis and Dunn statistical tests (5%). Extra samples of each group were made to obtain profilometry and scanning electron microscopy (SEM).

Result: Zirconia-cement bond strength was affected by the ceramic surface treatments (p = 0.001). G10-5s (2.71 MPa) recorded the highest bond strength values, followed by the Co (2.05 MPa) while G5 groups had the lowest bond value. Adhesive failure of the samples predominated. The image analysis revealed G5 groups seem to have a lower roughness when compared to groups treated by 10% HF. The creation of pores in the low-fusing porcelain glass layer surface occurred only when 10% HF was used.

Conclusion: The low-fusing porcelain glass layer application was able to overcome the sandblasting and obtain a greater adhesive bond to the resinous cement, however, only when 10% HF was used for an interval of 5 seconds.

Keywords

Zirconia, glaze, adhesion, surface treatment

Resumo

Resumo: Introdução: Apesar de ser uma das cerâmicas mais estudadas atualmente, a zircônia ainda não possui um protocolo bem definido para uma cimentação adesiva.

Objetivo: Avaliar a influência de diferentes tempos de condicionamento e concentrações do ácido fluorídrico (AF) na superfície da zirconia e na resistência de união entre uma cerâmica Y-TZP vitrificada e um cimento resinoso.

Material e método: Os tratamentos de superfície foram: jateamento com óxido de alumínio revestido com sílica (Co); aplicação de glaze + condicionamento com AF 5% por 5s (G5-5s), 10s (G5-10s) ou 20s (G5-20s); aplicação de glaze + condicionamento com AF 10% por 5s (G10-5s), 10 (G10-10s) ou 20s (G10-20s). Em seguida, cilindros de cimento (3,3 × 3,3mm) para teste de cisalhamento foram feitos em todos os espécimes. Os espécimes foram submetidos a 6000 ciclos térmicos antes do teste de adesão. As fraturas foram analisadas por estereomicroscópio. Os dados foram analisados ​​estatisticamente por Kruskal-Wallis e Dunn (5%). Amostras extra de cada grupo foram feitas para realização de perfilometria e microscopia eletrônica de varredura (MEV).

Resultado: A resistência de união zircônia-cimento foi afetada pelos tratamentos de superfície (p = 0,001). Os grupos G10-5s (2,71 MPa) registraram os maiores valores de resistência de união, seguidos pelos Co (2,05 MPa), enquanto os grupos G5 apresentaram o menor valor de união. Falhas adesivas foram predominantes. As análises por imagem revelaram que os grupos G5 parecem ser menos rugosos quando comparados aos grupos tratados com AF 10%. A criação de poros na superfície vítrea (glaze) ocorreu apenas quando foi utilizado AF 10%.

Conclusão: A aplicação de camada de vidro de porcelana de baixa fusão foi capaz de superar o jateamento e obter uma maior adesão adesiva ao cimento resinoso, no entanto, somente quando foi utilizado 10% de HF por um intervalo de 5 segundos.
 

Palavras-chave

Zirconia, glaze, adesão, tratamento de superfície

References

Moradabadi A, Roudsari SE, Yekta BE, Rahbar N. Effects of surface treatment on bond strength between dental resin agent and zirconia ceramic. Mater Sci Eng C Mater Biol Appl. 2014 Jan;34:311-7. http://dx.doi.org/10.1016/j.msec.2013.09.015. PMid:24268263.

Mota YA, Cotes C, Carvalho RF, Machado JPB, Leite FPP, Souza ROA, et al. Monoclinic phase transformation and mechanical durability of zirconia ceramic after fatigue and autoclave aging. J Biomed Mater Res B Appl Biomater. 2017 Oct;105(7):1972-7. http://dx.doi.org/10.1002/jbm.b.33720. PMid:27312806.

Cavalcanti AN, Foxton RM, Watson TF, Oliveira MT, Giannini M, Marchi GM. Y-TZP ceramics: key concepts for clinical application. Oper Dent. 2009 May-Jun;34(3):344-51. http://dx.doi.org/10.2341/08-79. PMid:19544825.

Attia A. Bond strength of three luting agents to zirconia ceramic: influence of surface treatment and thermocycling. J Appl Oral Sci. 2011 Aug;19(4):388-95. http://dx.doi.org/10.1590/S1678-77572011005000015. PMid:21710091.

Ntala P, Chen X, Niggli J, Cattell M. Development and testing of multi-phase glazes for adhesive bonding to zirconia substrates. J Dent. 2010 Oct;38(10):773-81. http://dx.doi.org/10.1016/j.jdent.2010.06.008. PMid:20600558.

Feitosa SA, Patel D, Borges AL, Alshehri EZ, Bottino MA, Özcan M, et al. Effect of cleansing methods on saliva-contaminated zirconia: an evaluation of resin bond durability. Oper Dent. 2015 Mar-Apr;40(2):163-71. http://dx.doi.org/10.2341/13-323-L. PMid:25136900.

Martins ARM, Gotti VB, Shimano MM, Borges GA, Gonçalves LS. Improving adhesion between luting cement and zirconia-based ceramic with an alternative surface treatment. Braz Oral Res. 2015;29(1):54. http://dx.doi.org/10.1590/1807-3107BOR-2015.vol29.0054. PMid:25859635.

Arai M, Takagaki T, Takahashi A, Tagami J. The role of functional phosphoric acid ester monomers in the surface treatment of yttria-stabilized tetragonal zirconia polycrystals. Dent Mater J. 2017 Mar;36(2):190-4. http://dx.doi.org/10.4012/dmj.2016-060. PMid:28111385.

Moezzizadeh M, Nojedehian H, Valizadeh Haghi H. Effect of bioglass and silica coating of zirconia substrate on its bond strength to resin cement. Dent Mater J. 2017 Jan;36(1):54-62. http://dx.doi.org/10.4012/dmj.2015-382. PMid:27928098.

Özcan M, Yetkiner E. Could readily silanized silica particles substitute silica coating and silanization in conditioning zirconium dioxide for resin adhesion? J Adhes Sci Technol. 2016;30(2):186-93. http://dx.doi.org/10.1080/01694243.2015.1095628.

Vu VT, Oh GJ, Yun KD, Lim HP, Kim JW, Nguyen TPT, et al. Acid etching of glass-infiltrated zirconia and its biological response. J Adv Prosthodont. 2017 Apr;9(2):104-9. http://dx.doi.org/10.4047/jap.2017.9.2.104. PMid:28435619.

Vanderlei A, Bottino MA, Valandro LF. Evaluation of resin bond strength to yttria-stabilized tetragonal zirconia and framework marginal fit: comparison of different surface conditionings. Oper Dent. 2014 Jan-Feb;39(1):50-63. http://dx.doi.org/10.2341/12-269-L. PMid:23586656.

Amaral M, Belli R, Cesar PF, Valandro LF, Petschelt A, Lohbauer U. The potential of novel primers and universal adhesives to bond to zirconia. J Dent. 2014 Jan;42(1):90-8. http://dx.doi.org/10.1016/j.jdent.2013.11.004. PMid:24246687.

Dias de Souza GM, Thompson VP, Braga RR. Effect of metal primers on microtensile bond strength between zirconia and resin cements. J Prosthet Dent. 2011 May;105(5):296-303. http://dx.doi.org/10.1016/S0022-3913(11)60055-3. PMid:21530754.

Papia E, Zethraeus J, Ransbäck PÅ, Wennerberg A, Vult von Steyern P. Impaction-modified densely sintered yttria-stabilized tetragonal zirconium dioxide: methodology, surface structure, and bond strength. J Biomed Mater Res B Appl Biomater. 2012 Apr;100(3):677-84. http://dx.doi.org/10.1002/jbm.b.31992. PMid:22278954.

Miranda JS, Malta NV, de Carvalho RLA, Souza ROA, Machado JPB, Leite FPP. Which low-fusing porcelain glaze treatment technique is better to promote a vitreous surface on Y-TZP ceramic? Rev Odonto Ciênc. 2018 Jul;32(4):174-9. http://dx.doi.org/10.15448/1980-6523.2017.4.28749.

Antunes MCF, Miranda JS, Carvalho RLA, Carvalho RF, Kimpara ET, Assunção e Souza RO, et al. Can low-fusing glass application affect the marginal misfit and bond strength of Y-TZP crowns? Braz Oral Res. 2018;32(0):e34. http://dx.doi.org/10.1590/1807-3107bor-2018.vol32.0034. PMid:29742232.

Yamamoto LT, Rodrigues VA, Dornelles LS, Bottino MA, Valandro LF, Melo RM. Low-fusing porcelain glaze application on 3y-tzp surfaces can enhance zirconia-porcelain adhesion. Braz Dent J. 2016 Sep-Oct;27(5):543-7. http://dx.doi.org/10.1590/0103-6440201601014. PMid:27982231.

Campos F, Valandro LF, Feitosa SA, Kleverlaan CJ, Feilzer AJ, de Jager N, et al. Adhesive cementation promotes higher fatigue resistance to zirconia crowns. Oper Dent. 2017 Mar/Apr;42(2):215-24. http://dx.doi.org/10.2341/16-002-L. PMid:27892840.

Bottino MA, Snellaert A, Bergoli CD, Özcan M, Bottino MC, Valandro LF. Effect of ceramic etching protocols on resin bond strength to a feldspar ceramic. Oper Dent. 2015 Mar-Apr;40(2):E40-6. http://dx.doi.org/10.2341/13-344-L. PMid:25535782.

Usumez A, Hamdemirci N, Koroglu BY, Simsek I, Parlar O, Sari T. Bond strength of resin cement to zirconia ceramic with different surface treatments. Lasers Med Sci. 2013 Jan;28(1):259-66. http://dx.doi.org/10.1007/s10103-012-1136-x. PMid:22718473.

Wandscher VF, Prochnow C, Rippe MP, Dorneles LS, Callegari GL, Baldissara P, et al. Retentive strength of y-tzp crowns: comparison of different silica coating methods on the intaglio surfaces. Oper Dent. 2017 Sep-Oct;42(5):E121-33. http://dx.doi.org/10.2341/16-090-L. PMid:28829934.

Zhao L, Jian YT, Wang XD, Zhao K. Bond strength of primer/cement systems to zirconia subjected to artificial aging. J Prosthet Dent. 2016 Nov;116(5):790-6. http://dx.doi.org/10.1016/j.prosdent.2016.03.020. PMid:27312655.

Anami LC, Lima JM, Corazza PH, Yamamoto ET, Bottino MA, Borges AL. Finite element analysis of the influence of geometry and design of zirconia crowns on stress distribution. J Prosthodont. 2015 Feb;24(2):146-51. http://dx.doi.org/10.1111/jopr.12175. PMid:24975118.
 

5c743f250e88257d27da818c rou Articles
Links & Downloads
1807-2577 (Electronic)
Rev. odontol. UNESP ©2024 All rights reserved.

Rev. odontol. UNESP

Share this page
Page Sections