Revista de Odontologia da UNESP
https://revodontolunesp.com.br/article/doi/10.1590/1807-2577.02020
Revista de Odontologia da UNESP
Original Article

Different bonding agents effect on adhesive bond strength: lithium disilicate glass ceramic

Efeito de diferentes agentes de união na cimentação adesiva em superfície cerâmica de dissilicato de lítio

Marcos Daniel Septímio LANZA; Walisson Arthuso VASCONCELLOS; Giovani Lana Peixoto de MIRANDA; Rogéli Tibúrcio Ribeiro da Cunha PEIXOTO; Lincoln Dias LANZA

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Abstract

Abstract: Introduction: The silanization of the ceramic surface prior to applying the adhesive and/or resinous materials plays an important role in bond strength. Nowadays, a new family of adhesive systems has been introduced into the market, aiming to simplify the technique of adhesive procedures during cementation.

Objective: To investigate the effectiveness of different bonding agents containing silane and primer on Lithium Disilicate Glass Ceramic (LD) surface by shear bond strength tests.

Material and method: 130 LD ceramic blocks were included in acrylic resin, polished and washed in ultrasound for 10 minutes. The specimens were divided into 2 groups according to surface treatment: Polished Surface (PS); Hydrofluoric Acid 9.5% - 20s (HF). Each group was divided into 5 subgroups (n = 13) according to bonding agent type: metallic primer containing MDP (ZPrimePlus, Bisco Inc); two traditional silanes (MonobondPlus, IvoclarVivadent / Porcelain Prime, Bisco Inc.); mixture of silane and resin (Kerr Silane, Kerr); mixture of silane and universal adhesive (Single-bond Universal, 3M Espe). The specimens were mounted in a standard device for shear testing (UltradentBonding Assembly), cemented with dual resin cement (RelyX UltimateTM, 3M Espe.) and photo-polymerized for 20s. The samples were tested after 24 hours and 3 months of storage in distilled water at ±36 °C. The data were analyzed by 3-Way Anova and Tukey's test (α = 5%).

Result: Shear bond strength (SBS) was significantly influenced by surface treatment, bonding agent used and storage (p <0.001).

Conclusion: Adequate adhesive bond strength to Lithium Disilicate Glass Ceramic can be obtained with traditional silanes, combined with HF acid pretreatment surface.

Keywords

Adhesion, adhesive strength, lithium disilicate glass ceramic, resin cement, silanes

Resumo

Resumo: Introdução: A silanização da superfície cerâmica antes da aplicação do adesivo e/ou materiais resinosos desempenha um papel importante na resistência adesiva. Atualmente, uma nova família de sistemas adesivos foi introduzida no mercado, visando simplificar a técnica dos procedimentos adesivos durante a cimentação.

Objetivo: Investigar a eficácia de diferentes soluções contendo silano e primer na superfície de cerâmicas de Dissilicato de Lítio (DLT) por meio de testes de resistência adesiva por cisalhamento.

Material e método: 130 blocos cerâmicos DLT foram incluídos em resina acrílica, polidos e lavados em ultra-som por 10 minutos. Os espécimes foram divididos em 2 grupos de acordo com tratamento de superfície: Superfície Polida (PS); Ácido Hidro-Fluorídrico 9,5% - 20s (HF). Cada grupo foi dividido em 5 sub-grupos (n = 13) de acordo com o tipo de primer/silano: primer metálico contendo MDP (ZprimePlus, Bisco Inc); dois silanos tradicionais (MonobondPlus, IvoclarVivadent / Porcelain Prime, Bisco Inc.); mistura de silano e resina (Kerr Silane, Kerr); mistura de silano e adesivo universal (Single-bond Universal, 3M Espe). Os espécimes foram montados em um dispositivo padrão (UltradentBonding Assembly) para teste de cisalhamento Bisco Shear Bond Tester), cimentados com cimento resinoso dual (RelyX UltimateTM, 3M Espe.) e foto-polimerizados por 20s. O teste foi realizado após o período de: 24 horas e 3 meses de armazenamento em água destilada à ±36 °C. Os dados foram analisados por 3-Way Anova e Teste de Tukey (α=5%).

Resultado: A resistência adesiva ao cisalhamento (SBS) foi significativamente influenciada pelo tipo de tratamento da superfície, pelo tipo de agente de união utilizado e pelo armazenamento (p<0,001).

Conclusão: Adequada resistência adesiva pode ser obtida com silanos tradicionais, combinados com o pré-tratamento de superfície com ácido HF.
 

Palavras-chave

Adesão, resistência adesiva, dissilicato de lítio, cimento resinoso, silano

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Submitted date:
03/27/2020

Accepted date:
07/06/2020

5f5296df0e8825b4657dc2e4 rou Articles
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